LC Multiresidue Pesticide Standard #7 on Raptor™ ARC-18 by LC-MS/MS

PeakstR (min)Precursor IonProduct Ion 1Product Ion 2
1.Fenpropimorph3.43304.2147.157.2
2.Spirotetramat4.57374.2330.3302.2
3.Spinosyn A5.03732.6142.098.1
4.Spinosyn D5.30746.5142.098.1
5.Spinetoram5.37748.5142.298.1
6.Emamectin benzoate B1b5.57872.4158.2126.1
7.Emamectin benzoate B1a5.74886.5158.1126.1
8.Spiromesifen6.19371.1273.1255.1
9.Spirodiclofen6.33411.1313.071.2
image
LC_FF0549
ColumnRaptor™ ARC-18 (cat.# 9314A12)
Dimensions:100 mm x 2.1 mm ID
Particle Size:2.7 µm
Temp.:50 °C
SampleLC multiresidue pesticide standard #7 (cat.# 31978)
Diluent:Water
Conc.:20 ng/mL
Inj. Vol.:5 µL
Mobile Phase
A:Water + 2 mM ammonium formate + 0.2% formic acid
B:Methanol + 2 mM ammonium formate + 0.2% formic acid
Time (min)Flow (mL/min)%A%B
0.000.4955
2.000.44060
4.000.42575
6.000.40100
7.000.40100
7.010.4955
9.500.4955
DetectorWaters Xevo TQ-S
Ion Source:Waters Zspray™ ESI
Ion Mode:ESI+
Mode:MRM
InstrumentWaters
NotesAutosampler Temperature = 5 °C
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