Carbamates on Ultra Carbamate

Peaks
1.Aldicarb sulfone
2.Aldicarb sulfoxide
3.Oxamyl
4.Methomyl
5.3-Hydroxycarbofuran
Peaks
6.Aldicarb
7.Propoxur
8.Carbofurane
9.Carbaryl
10.Methiocarb
11.BDMC (IS)
image
LC_FF0473
ColumnUltra Carbamate (cat.# 9177352)
Dimensions:50 mm x 2.1 mm ID
Particle Size:3 µm
Pore Size:100 Å
Temp.:ambient
Sample531.1 Carbamate Pesticide Calibration Mixture (cat.# 32273)
4-bromo-3,5-dimethylphenyl-N-methylcarbamate (BDMC) (cat.# 32274)
Diluent:methanol
Conc.:50 µg/mL
Inj. Vol.:1 µL
Mobile Phase
A:2 mM ammonium acetate:methanol (v/v, 90/10)
B:2 mM ammonium acetate:methanol (v/v, 10/90)
Time (min)%A%B
0.008020
200100
250100
Flow:0.2 mL/min
DetectorLECO Unique® TOFMS
Run Length:25 min
Ionization Source Type:high flow ESI
Ion Mode:positive
Desolvation Temp.:130 °C
Nebulizing Pressure:100 kPa
Desolvation Gas (N2):4 L/min
Interface Temp.:120 °C
Nozzle Voltage:62 V
Capillary Voltage:2.75 kV
InstrumentAgilent 1100
AcknowledgementLECO Corporation
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EPA 531.1

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EPA 531

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