Residual Solvents (Class 2 - Mixture A) on Stabilwax (G16)

Peaks
1.Cyclohexane
2.Methylcyclohexane
3.trans-1,2-Dichloroethene
4.Tetrahydrofuran
5.Methanol
6.Dichloromethane
7.cis-1,2-Dichloroethene
Peaks
8.Acetonitrile
9.Toluene
10.1,4-Dioxane
11.Ethyl benzene
12.p-Xylene
13.m-Xylene
14.o-Xylene
15.Chlorobenzene
image
GC_PH00952
ColumnStabilwax®, 30 m, 0.32 mm ID, 0.25 µm (cat.# 10624)
SampleResidual solvents class 2 - mix A (cat.# 36271)
in 20 mL headspace vial (cat.# 24685)
Diluent:Water
Injection
Inj. Vol.:1,000 µL headspace-syringe split (split ratio 5:1)
Liner:2 mm splitless (cat.# 20712)
Inj. Temp.:140 °C
Headspace-Syringe
Instrument:Overbrook Scientific HT200H
Syringe Temp.:100 °C
Sample Temp.:80 °C
Sample Equil. Time:45 min
Inj. Speed:8
Inj. Dwell:5 sec.
Oven
Oven Temp.:50 °C (hold 20 min) to 165 °C at 6 °C/min (hold 20 min)
Carrier GasHe, constant flow
Flow Rate:2.15 mL/min
Linear Velocity:35.2 cm/sec
DetectorFID @ 250 °C
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