Volatile Amine Test Mix on Rtx-Volatile Amine (60 m x 0.32 mm ID)

PeakstR (min)
1.Pyridine5.29
2.1,2-Butanediol6.15
3.Nonane8.14
4.Diethylenetriamine11.82
5.Diethanolamine12.69
6.2-Nonanol15.81
7.2,6-Dimethylamine21.62
8.Dodecane22.73
image
GC_PC1228
ColumnRtx-Volatile Amine, 60 m, 0.32 mm ID (cat.# 18078)
SampleVolatile amine column test mix (cat.# 35008)
Diluent:Methanol:dichloromethane (50:50)
Conc.:900-1,800 µg/mL snap and shoot
Injection
Inj. Vol.:1 µL split (split ratio 17.8:1)
Liner:Premium 4 mm single taper w/wool (cat.# 23303.1)
Inj. Temp.:250 °C
Split Vent Flow Rate:60 mL/min
Oven
Oven Temp.:160 °C (hold 21 min) to 290 °C at 40 °C/min (hold 10 min)
Carrier GasHe, constant flow
Flow Rate:3.4 mL/min
DetectorFID @ 300 °C
Make-up Gas Flow Rate:30 mL/min
Make-up Gas Type:N2
Data Rate:50 Hz
InstrumentAgilent/HP6890 GC
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