GC Multiresidue Pesticide Standard #7-HME on Rxi-5ms by GC-MS

PeakstR (min)
1.2-Phenylphenol10.17
2.Chlorpropham12.02
3.Metalaxyl15.38
4.DCPA methyl ester (Chlorthal-dimethyl)16.33
5.Chlozolinate17.05
PeakstR (min)
6.Fluazifop-P-butyl18.84
7.Chlorobenzilate19.02
8.Carfentrazone ethyl19.84
9.Bromopropylate21.12
10.Acequinocyl24.54
image
GC_FS0606
ColumnRxi®-5ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423)
SampleGC multiresidue pesticide standard #7-HME (cat.# 32569)
Diluent:Toluene
Conc.:100 µg/mL
Injection
Inj. Vol.:1 µL split (split ratio 50:1)
Liner:Premium 4.0 mm ID Precision® inlet liner w/wool (cat.# 23305.1)
Inj. Temp.:250 °C
Oven
Oven Temp.:90 °C (hold 1 min) to 330 °C at 8.5 °C/min (hold 5 min)
Carrier GasHe, constant flow
Flow Rate:1.4 mL/min
DetectorMS
Mode:Scan
Scan Program:
GroupStart Time
(min)
Scan Range
(amu)
Scan Rate
(scans/sec)
1555-5507
Transfer Line Temp.:290 °C
Analyzer Type:Quadrupole
Source Temp.:325 °C
Electron Energy:70 eV
Solvent Delay Time:5 min
Ionization Mode:EI
InstrumentThermo Scientific TSQ 8000 Triple Quadrupole GC-MS
NotesReconstructed chromatogram from select ions.
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