NIST SRM 1975, Diesel Particulate Extract, on Rxi-PAH

Peaks
1.Naphthalene-D8
2.Naphthalene
3.2-Methylnaphthalene
4.Biphenyl
5.Acenaphthylene
6.Acenaphthene-D10
7.Acenaphthene
8.Fluorene
9.Dibenzothiophene
10.Phenanthrene-D10
11.Phenanthrene
12.Anthracene
13.4H-Cyclopenta[def]phenanthrene
14.Fluoranthene
15.Pyrene
16.Benzo[ghi]fluoranthene
17.Benzo[c]phenanthrene
18.Benz[a]anthracene
19.Chrysene-D12
Peaks
20.Triphenylene
21.Chrysene
22.Benzo[b]fluoranthene
23.Benzo[k]fluoranthene
24.Benzo[j]fluoranthene
25.Benzo[e]pyrene
26.Benzo[a]pyrene-D12
27.Benzo[a]pyrene
28.Perylene-D12
29.Dibenzo[a,j]anthracene
30.Dibenzo[a,c]anthracene
31.Indeno[1,2,3-cd]pyrene
32.Dibenz[a,h]anthracene
33.Benzo[b]chrysene
34.Picene
35.Benzo[ghi]perylene
36.Dibenzo[b,k]fluoranthene
37.Coronene-D12
38.Coronene
image
GC_EV1392
ColumnRxi-PAH, 60 m, 0.25 mm ID, 0.10 µm (cat.# 49317)
SampleNIST SRM 1975
Diluent:Dichloromethane
Injection
Inj. Vol.:1 µL split (split ratio 10:1)
Liner:Premium 4 mm Precision liner w/wool (cat.# 23305.1)
Inj. Temp.:275 °C
Split Vent Flow Rate:19.5 mL/min
Oven
Oven Temp.:110 °C (hold 1.6 min) to 210 °C at 24 °C/min to 295 °C at 1.9 °C/min to 350 °C at 3.7 °C/min (hold 6 min)
Carrier GasHe, constant flow
Flow Rate:1.95 mL/min
DetectorMS
Mode:SIM
SIM Program:
GroupStart Time
(min)
Ion(s) (m/z)Dwell (ms)
13.09102.1, 108.1, 128.1, 136.2 40
25.69115.1, 142.1 40
36.2376.1, 141.1, 154.1, 156.2 40
46.9575.6, 76.1, 91.1, 152.1, 153.1, 155.1, 162.2, 170.2 20
57.9382.4, 165.1 40
69.19139.1, 152.1, 160.2, 178.1, 184.1, 188.2 40
711.7894.6, 165.1, 190.1, 192.1 40
814.19101.1, 202.1 40
916.60101.1, 202.1 40
1018.4992.1, 184.1 40
1119.58108, 216 40
1222.3196.1, 212.2 40
1324.92113.1, 226.1, 228.1 40
1426.27113.1, 114.0, 120.1, 226.1, 228.1, 240.1 40
1528.75154.1, 252.1 35
1630.62119.8, 242.2 40
1735.29126.1, 252.1 40
1838.56125.1, 252.1 40
1939.23126.1, 252.1 40
2040.71125.1, 126.1, 132.1, 252.1, 264.1 40
2142.91125, 132.2, 252.1, 264.1 40
2244.35252.1, 268.1 40
2348.41139.1, 139.5, 278.1, 279.1 40
2452.13139.1, 139.5, 278.1, 279.1 40
2553.70138.1, 139.1, 278.1 40
2654.97138.1, 276.1 40
2755.92138.1, 276.1 40
2857.04132.6, 267.1 40
2959.69151.0, 302.1 40
3063.27150, 151, 156.1, 300.1, 302.1, 312.1 40
3164.78151.0, 302.1 40
Transfer Line Temp.:330 °C
Analyzer Type:Quadrupole
Source Type:Extractor
Extractor Lens:9 mm ID
Source Temp.:350 °C
Quad Temp.:200 °C
Solvent Delay Time:3 min
Tune Type:DFTPP
Ionization Mode:EI
InstrumentAgilent 7890B GC & 5977A MSD
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